The evolution of sol–gel chemistry as a technique for
The evolution of sol–gel chemistry as a technique for materials synthesis A E Danks S R Hall and Z Schnepp Mater Horiz 2016 3 91 DOI 10 1039/C5MH00260E This article is licensed under a Creative Commons Attribution 3 0 Unported Licence You can use material from this article in other publications without requesting further permissions from the RSC provided that the correct
Get PricePreparation of alumina films from a new sol–gel route
sol–gel etc Among these the sol–gel method is an emer ging route with high promise for very homogeneous films which can be formed at relatively low temperatures Generally the aluminum alkoxides such as aluminum sec butoxide and aluminum iso propoxide are chosen to prepare alumina films by the sol–gel method 6–8
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The nanostructured γ and α alumina powders were synthesized by sol gel and co precipitation methods and properties of the powders were studied by XRD SEM TEM BET and FTIR The results showed that both γ and α phases were formed in the lower temperature in precipitation method compared to sol gel The size of spherical α alumina synthesized by sol gel was 10–15 nm
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High alumina castables a comparison among various sol gel May 11 2017 A comparison among various sol gel bonding systems has been done for high alumina castable refractory Four different sol systems namely alumina boehmite mullite and spinel have been synthesized and used individually as sole binder in high alumina castable system with
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Improved sol gel spinel MgAl 2 O 4 coatings on graphite for application in carbon containing high alumina castables J Sol Gel Sci Technol 56 2010 pp 6674 CrossRef View Record in Scopus Google Scholar
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Instead the primers and topcoats have VOC contents of 340 and 420 g/l respectively in comparison with the aqueous sol gel solutions suitable for spray coating on aluminum substrates which have a VOC content of 100–200 g/l On the other hand the method allows to obtain thin films of sub micrometer thickness with high purity in multiple
Get Pricesynthesis of nano alumina powder using an aqueous sol–gel
There are some limitations in all aforementioned methods Among the various synthesis methods sol–gel method is the most promising and thus has been widely investigated because it produces solid particles of high purity and high specific surface area It is known that aluminum alkoxides are very popular for processing of alumina
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Furthermore the performance of various high alumina aggregates was evaluated and the results confirm that in comparison with silica sol the microsilica gel bonded refractory NCCs exhibit improved set behaviour and green strength download full Article PDF Keywords no cement castable silica sol microsilica gel bond additive References
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powders with high purity by various routes such as precipitation sol gel and hydrothermal methods Among these methods precipitation is the most commonly used method not only because it can produce high quality powders but also it is cheap The precipitation of aluminum depends on several factors as temperature and pH
Get PriceDensification of Ca Doped Alumina Nanopowders
Densification of Ca doped alumina nanopowders prepared by a new sol gel route with seeding Atsushi Odaka a Tomohiro Yamaguchi a Takayuki Fujita b Seiichi Taruta a and Kunio Kitajima a a Department of Chemistry and Material Engineering Faculty of Engineering Shinshu University 4 17 1 Wakasato Nagano shi
Get PricePreparation of alumina films from a new sol–gel route
sol–gel etc Among these the sol–gel method is an emer ging route with high promise for very homogeneous films which can be formed at relatively low temperatures Generally the aluminum alkoxides such as aluminum sec butoxide and aluminum iso propoxide are chosen to prepare alumina films by the sol–gel method 6–8
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Among the other sol bonding systems mainly alumina mullite magnesia and spinel sols are tested for refractory castables But there is not enough literature available on such studies The major hindrances for such applications are various processing difficulties such as a lower solid content of sol leading to poor bonding activity weak
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The iterature also shows some studies on the use of nanoparticles prepared by the sol gel process and then further used in high alumina castables Alumina mullite spinel etc nanopowders prepared by the sol gel technique are used 101–103 in cement bonded alumina castables to improve the properties But the exact effect of these individual nanoparticles on the alumina castable is difficult
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High alumina castables a comparison among various sol gel bonding systems Akhilesh K Singh and Ritwik Sarkar Journal of the Australian Ceramic Society 53 pp 553–567 2017 69
Get PriceBinders for Refractory Castables An Overview SpringerLink
Fine gel particles make for better sintering of the castable result in ceramic bond formation at a lower temperature 43 44 50 53 and produce better properties compared to cement bonded ones 37 38 54 Figure 3 Phase analysis of fired silica sol containing high alumina castable 49
Get PriceThe evolution of sol–gel chemistry as a technique for
The evolution of sol–gel chemistry as a technique for materials synthesis A E Danks S R Hall and Z Schnepp Mater Horiz 2016 3 91 DOI 10 1039/C5MH00260E This article is licensed under a Creative Commons Attribution 3 0 Unported Licence You can use material from this article in other publications without requesting further permissions from the RSC provided that the correct
Get PriceStudy on the effect of different sols on high alumina
Among the various unshaped refractories castables lead in all the areas of research development manufacturing and application Keywords sol gel high alumina castable alumina sol boehmite sol mullite sol spinel sol characterization ix C 2 5 Sol Gel bonding in castables
Get PriceSol–gel mullite as the self bonding material for
The sol–gel mullite as the permanent binder yields density up to 2 48 g/cc The room temperature flexural strength 172 kg/cm 2 and compressive strength 785 kg/cm 2 of the self bonded fused mullite are comparable to that of the conventional clay/alumina bonded mullite products
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High alumina cement and silica sol were used at Among the various unshaped refractories castables lead in all the areas of research development manufacturing and application Physical mechanical chemical and through the sol gel route appeared in the industry which opened a new horizon for refractory
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Modified sol–gel method has been recently applied for alumina nanostructures using various soft templates such as P123 F127 Triethanolamine TEA and etc 19 20 21 22 23 During the last decade there have been enormous advances in synthesis of high surface area MA and OMA by sol gel method using different types of soft templates 16 24
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Among alternate bonding materials development of sol gel technique has opened a new horizon in bonding system for refractory technologists The principle behind sol gel bonding is the formation of a 3 dimensional network gel of particles that surrounds the refractory materials and which on subsequent heating develop strength by formation of
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sol–gel process will be our major focus which is easy to prepare and can be used to coat ceramic powders with high dielectric constant and to develop various types of dielectric composites Alumina thin films were prepared via sol–gel wet chem istry route usingorganicor inorganicprecursors In
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Sol gel based method assisted by Pluronic P123 has been employed to successfully synthesize mesoporous alumina MA with high surface area 363 4 m2 g−1 large pore volume 0 65 cm3 g−1 and narrow pore size distribution 7 42 nm An optimization study was performed using response surface methodology RSM to design the experiments
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product in alumina castables bonded with high purity aluminate cement It is believed that CA 6 is most readily formed in alumina castables when using CA 2 as a precursor 7 Alumina A is sometimes present as an addition and this is especially true in the case of 80 alumina calcium aluminate cements 3 Calcium aluminate cement hydration
Get PriceInfluence of gel derived nanocrystalline spinel in a high
A newer class of spinel alumina castable was fabricated by incorporating 8 0wt of modified spinel additives synthesized via sol–gel and coprecipitat
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The ethanol dehydration to ethylene over alumina catalysts prepared by solvothermal and sol gel methods was investigated Also a commercial alumina was used for comparison purposes The results showed that the catalytic activity depends on the properties of catalyst derived from different preparation methods and reaction temperature The alumina synthesized by solvothermal method exhibited
Get PriceComparison of Urea and Citric Acid Complexing Agents and
A sol gel method based on the Pechini process was used to synthesize different phases of alumina nanoparticles using a polymeric precursor with Aluminum nitrate The emphasis was on investigating the effect of two different complexing agents urea and citric acid on the structural properties particle size and phase transformation during the heat treatment that was studied by XRD
Get PriceStudy on The Effect of Different Sols on High Alumina
Among alternate bonding materials development of sol gel technique has opened a new horizon in bonding system for refractory technologists The principle behind sol gel bonding is the formation of a 3 dimensional network gel of particles that surrounds the refractory materials and which on subsequent heating develop strength by formation of
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The excellent properties of this catalyst were also attributed to the special porous structure and high surface area of the aerogel maintained by the supercritical drying this work we investigate various sol gel processes and drying methods including the application of chelating agent and freeze drying for producing Fe Mo Al 2 O 3 sol gel
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Ever increasing demand and application of unshaped refractories replacing shaped ones have inspired the scientists and manufacturers to investigate these materials in depth for further improving the quality and performance Among the various unshaped refractories castables lead in all the areas of research development manufacturing and application
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Ever increasing demand and application of unshaped refractories replacing shaped ones have inspired the scientists and manufacturers to investigate these materials in depth for further improving the quality and performance Among the various unshaped refractories castables lead in all the areas of research development manufacturing and application
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High alumina castables a comparison among various sol gel bonding systems Akhilesh K Singh and Ritwik Sarkar Journal of the Australian Ceramic Society 53 2 pp 553–567 2017 69 Hydroxyapatite based machinable bioceramic an in depth investigation on drilling parameters and bioactivity Rupita Ghosh Ritwik Sarkar Soumitra Paul
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A documentary study on alumina extraction processes from materials other than high grade bauxite ores has been carried out at the request of the B R G M mis sion in Saudi Arabia Processes which are applicable to alumino silicates and related materials high silica high iron bauxites have been exclusively considered in this study
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